5WEE
Crystal structure of HpVAL4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2016-08-15 |
Detector | RIGAKU RAXIS HTC |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 |
Unit cell lengths | 49.560, 61.565, 74.819 |
Unit cell angles | 111.59, 90.14, 113.47 |
Refinement procedure
Resolution | 40.883 - 1.990 |
R-factor | 0.1788 |
Rwork | 0.176 |
R-free | 0.22800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1u53 |
RMSD bond length | 0.007 |
RMSD bond angle | 0.974 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((dev_2722)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 52.700 |
High resolution limit [Å] | 1.990 |
Rmerge | 0.139 |
Rpim | 0.057 |
Number of reflections | 48537 |
<I/σ(I)> | 18 |
Completeness [%] | 95.4 |
Redundancy | 7.2 |
CC(1/2) | 0.996 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 298 | 0.1M NaAcetate pH 4.5, 22.5% Poly PEG 0.3 -8kD |