Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE BM30A |
| Synchrotron site | ESRF |
| Beamline | BM30A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2001-04-29 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 44.860, 76.850, 78.890 |
| Unit cell angles | 90.00, 102.08, 90.00 |
Refinement procedure
| Resolution | 24.930 - 1.650 |
| R-factor | 0.1267 |
| Rwork | 0.123 |
| R-free | 0.15810 |
| Structure solution method | FOURIER SYNTHESIS |
| Starting model (for MR) | 1k07 |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.354 |
| Data reduction software | DENZO |
| Data scaling software | SCALA |
| Phasing software | AMoRE |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.740 |
| High resolution limit [Å] | 1.650 | 1.650 |
| Rmerge | 0.029 | 0.051 |
| Number of reflections | 61308 | 8838 |
| <I/σ(I)> | 21.9 | |
| Completeness [%] | 97.9 | 96.9 |
| Redundancy | 3.5 | 2.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 20% PEG4000, 0.2M ammonium sulfate, 0.010MM ZnCl2, pH 5.0 |
