5WCE
Caulobacter crescentus pol III beta
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | AREA DETECTOR |
Collection date | 2016-01-04 |
Detector | MARRESEARCH |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 83.855, 59.572, 86.490 |
Unit cell angles | 90.00, 92.89, 90.00 |
Refinement procedure
Resolution | 86.380 - 1.900 |
R-factor | 0.18884 |
Rwork | 0.187 |
R-free | 0.22624 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4tr8 |
RMSD bond length | 0.015 |
RMSD bond angle | 1.763 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 86.380 | 1.970 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.037 | 0.342 |
Rpim | 0.035 | 0.324 |
Number of reflections | 62720 | 5655 |
<I/σ(I)> | 19.9 | 2.1 |
Completeness [%] | 93.0 | 84.4 |
Redundancy | 1.9 | 1.8 |
CC(1/2) | 0.817 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.6 | 298 | PEG |