5W7M
Crystal structure of RoqN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-11-11 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9794 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 49.062, 100.838, 130.086 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.011 - 1.700 |
R-factor | 0.1847 |
Rwork | 0.182 |
R-free | 0.22520 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 0.913 |
Data scaling software | XSCALE |
Phasing software | CRANK2 |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 47.011 |
High resolution limit [Å] | 1.700 |
Rmerge | 0.059 |
Number of reflections | 35659 |
<I/σ(I)> | 20.63 |
Completeness [%] | 99.3 |
Redundancy | 6.5 |
CC(1/2) | 0.999 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.6 | 293 | PEG 3350, ethylene glycol, magnesium acetate |