5W6J
Agrobacterium tumefaciens ADP-glucose pyrophosphorylase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 80 |
Detector technology | CCD |
Collection date | 2015-04-15 |
Detector | MARRESEARCH |
Wavelength(s) | 0.98 |
Spacegroup name | P 1 |
Unit cell lengths | 93.439, 140.685, 228.490 |
Unit cell angles | 72.04, 78.19, 89.98 |
Refinement procedure
Resolution | 36.550 - 1.780 |
R-factor | 0.202 |
Rwork | 0.200 |
R-free | 0.22900 |
RMSD bond length | 0.007 |
RMSD bond angle | 0.763 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.810 |
High resolution limit [Å] | 1.780 | 4.830 | 1.780 |
Rmerge | 0.049 | 0.023 | 0.729 |
Rmeas | 0.067 | 0.032 | |
Rpim | 0.049 | 0.023 | 0.729 |
Total number of observations | 1967391 | ||
Number of reflections | 1003131 | ||
<I/σ(I)> | 8.2 | ||
Completeness [%] | 97.3 | 95.8 | 96.1 |
Redundancy | 2 | 2 | 2 |
CC(1/2) | 0.998 | 0.561 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 50mM HEPES pH 7.5, 1.5M Li2SO4 |