5W67
HLA-C*06:02 presenting VRSRR(ABA)LRL
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-10-05 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9537 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 44.065, 81.575, 116.098 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.197 - 2.300 |
R-factor | 0.1907 |
Rwork | 0.188 |
R-free | 0.23470 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4nt6 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.505 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.200 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Rpim | 0.090 | 0.420 |
Number of reflections | 19189 | 6072 |
<I/σ(I)> | 7.5 | 3.2 |
Completeness [%] | 99.7 | 99.9 |
Redundancy | 4 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 298 | 0.1M Na acetate pH 4.5 and 1.8 M ammonium citrate |