5W45
Crystal structure of APOBEC3H
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-06-11 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.99 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 46.749, 65.006, 65.540 |
Unit cell angles | 90.00, 90.08, 90.00 |
Refinement procedure
Resolution | 46.749 - 2.486 |
R-factor | 0.2136 |
Rwork | 0.211 |
R-free | 0.23480 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.002 |
RMSD bond angle | 0.551 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | PHENIX (1.12_2829) |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 279 | 0.2 M Na thiocyanate 4% PEG 20K |