5W3W
Crystal structure of SsoPox AsD6 mutant (V27A-Y97W-L228M-W263M) - open form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-02-02 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.00882 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 82.340, 105.010, 153.150 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.670 - 2.950 |
R-factor | 0.23194 |
Rwork | 0.229 |
R-free | 0.28841 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vc5 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.358 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 49.667 |
High resolution limit [Å] | 2.950 |
Rmerge | 0.066 |
Number of reflections | 28163 |
<I/σ(I)> | 12.89 |
Completeness [%] | 98.3 |
Redundancy | 3.77 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 20-30 % (w/v) PEG 8000 and 50 mM Tris-HCl buffer (pH 8) |