5W3T
Crystal structure of PopP2 in complex with IP6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-11-30 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9774 |
Spacegroup name | P 1 |
Unit cell lengths | 77.987, 78.956, 79.902 |
Unit cell angles | 103.36, 112.12, 111.54 |
Refinement procedure
Resolution | 66.349 - 2.150 |
R-factor | 0.1897 |
Rwork | 0.189 |
R-free | 0.24270 |
Structure solution method | SAD |
RMSD bond length | 0.006 |
RMSD bond angle | 0.969 |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 66.870 | 2.100 |
High resolution limit [Å] | 2.060 | 2.060 |
Rmerge | 0.066 | 1.159 |
Number of reflections | 75480 | |
<I/σ(I)> | 10.1 | 0.8 |
Completeness [%] | 93.6 | 94.1 |
Redundancy | 2.6 | 2.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 293 | 0.1 M HEPES (pH 7.5), 20% (v/v) PEG4000 and 10% (v/v) glycerol |