5W1K
JUNV GP1 CR1-10 Fab CR1-28 Fab complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-E |
Synchrotron site | APS |
Beamline | 21-ID-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-08-05 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 154.840, 132.230, 167.420 |
Unit cell angles | 90.00, 92.47, 90.00 |
Refinement procedure
Resolution | 49.350 - 3.990 |
R-factor | 0.239 |
Rwork | 0.237 |
R-free | 0.28800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5en2 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.150 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 49.350 | 49.350 | 4.230 |
High resolution limit [Å] | 3.990 | 11.680 | 3.990 |
Rmerge | 0.721 | 0.134 | 1.586 |
Rmeas | 0.857 | 0.160 | 1.886 |
Total number of observations | 194531 | ||
Number of reflections | 57195 | 2333 | 8957 |
<I/σ(I)> | 2.34 | 7.53 | 1.03 |
Completeness [%] | 99.1 | 97 | 97.6 |
Redundancy | 3.401 | 3.342 | 3.409 |
CC(1/2) | 0.796 | 0.988 | 0.465 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH MODE | 7.7 | 297 | 1.9 M AmSO4 pH 7.7 |