5W05
ANTI-TISSUE FACTOR ANTIBODY M59, A HUMANIZED VERSION OF 10H10
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-03-05 |
Detector | RIGAKU SATURN 944 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 43.380, 80.650, 112.160 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.640 |
R-factor | 0.18751 |
Rwork | 0.187 |
R-free | 0.20410 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4m7k |
RMSD bond length | 0.006 |
RMSD bond angle | 1.165 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.680 |
High resolution limit [Å] | 1.640 | 1.640 |
Rmerge | 0.040 | 0.179 |
Number of reflections | 45702 | 2034 |
<I/σ(I)> | 38 | 5.7 |
Completeness [%] | 93.1 | 56.4 |
Redundancy | 8.8 | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | 0.1 M MES PH 6.5, 16% PEG 3350, 0.2 M SODIUM FORMATE |