5VXN
Structure of two RcsB dimers bound to two parallel DNAs.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-G |
Synchrotron site | APS |
Beamline | 21-ID-G |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-06-16 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 0.97857 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 74.116, 113.231, 76.868 |
Unit cell angles | 90.00, 115.37, 90.00 |
Refinement procedure
Resolution | 56.615 - 3.375 |
R-factor | 0.202 |
Rwork | 0.199 |
R-free | 0.26830 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.556 |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 113.230 | 3.390 |
High resolution limit [Å] | 3.370 | 3.370 |
Rmerge | 0.100 | 0.600 |
Number of reflections | 15089 | |
<I/σ(I)> | 10.8 | 2.1 |
Completeness [%] | 93.0 | 100 |
Redundancy | 4.3 | 4.5 |
CC(1/2) | 0.990 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 293 | 0.2 M Sodium Chloride, 0.1 M HEPES, 25% PEG3350 |