5VXB
Crystal structure of Caulobacter crescentus ProXp-ala at 1.69 Angstrom
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-04-08 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.979180 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 62.042, 67.733, 62.927 |
Unit cell angles | 90.00, 118.62, 90.00 |
Refinement procedure
Resolution | 19.805 - 1.690 |
R-factor | 0.1673 |
Rwork | 0.166 |
R-free | 0.18960 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1vjf |
RMSD bond length | 0.007 |
RMSD bond angle | 0.792 |
Data reduction software | XDS (NA) |
Data scaling software | XDS (NA) |
Phasing software | PHASER (NA) |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.880 | 1.780 |
High resolution limit [Å] | 1.690 | 1.690 |
Rpim | 0.026 | 0.228 |
Number of reflections | 51097 | 7401 |
<I/σ(I)> | 16.3 | 3.3 |
Completeness [%] | 99.6 | 99 |
Redundancy | 6.7 | 6.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 0.005M Trisodium Citrate(pH5.6), 15% Glycerol, 25.5% w/v PEG4000 |