5VVP
HLA-B*57:03 presenting LSSPVTKSW
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-10-05 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.954 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 50.604, 81.838, 109.950 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.449 - 2.000 |
R-factor | 0.1709 |
Rwork | 0.169 |
R-free | 0.20170 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2rfx |
RMSD bond length | 0.004 |
RMSD bond angle | 0.833 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.1_1168) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 33.449 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.140 | 0.490 |
Number of reflections | 31614 | 4559 |
<I/σ(I)> | 10.2 | 3.7 |
Completeness [%] | 99.9 | 100 |
Redundancy | 5.4 | 5.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.4 | 298 | 12 -20 % PEG 4000, 0.2 M ammonium acetate and 0.1 M tri-sodium citrate pH 5.4 |