5VMN
Crystal structure of grouper iridovirus GIV66
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
| Synchrotron site | Australian Synchrotron |
| Beamline | MX1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2016-11-09 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9537 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 68.033, 68.033, 85.824 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 41.964 - 1.650 |
| R-factor | 0.1847 |
| Rwork | 0.183 |
| R-free | 0.21420 |
| Structure solution method | SAD |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.017 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | SHELXCD |
| Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 42.910 | 1.680 |
| High resolution limit [Å] | 1.650 | 1.650 |
| Rmerge | 0.057 | 2.395 |
| Number of reflections | 24871 | 1219 |
| <I/σ(I)> | 24.8 | 1.1 |
| Completeness [%] | 99.9 | 100 |
| Redundancy | 10 | 11.1 |
| CC(1/2) | 0.999 | 0.396 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 293 | 4.0 M sodium nitrate with 0.1 M sodium acetate pH 4.6 |
