5VLG
Crystal structure of EilR in complex with malachite green
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.2 |
Synchrotron site | ALS |
Beamline | 8.2.2 |
Temperature [K] | 100 |
Detector technology | AREA DETECTOR |
Collection date | 2014-10-14 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 100.145, 85.985, 102.275 |
Unit cell angles | 90.00, 101.69, 90.00 |
Refinement procedure
Resolution | 50.076 - 2.932 |
R-factor | 0.199 |
Rwork | 0.197 |
R-free | 0.24010 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.468 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | PHENIX ((dev_2650: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.076 |
High resolution limit [Å] | 2.930 |
Number of reflections | 36135 |
<I/σ(I)> | 6.8 |
Completeness [%] | 99.9 |
Redundancy | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2 M Tri-Sodium citrate, 20 % PEG 3350 |