Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 HF |
| Temperature [K] | 110 |
| Detector technology | IMAGE PLATE |
| Collection date | 2008-08-08 |
| Detector | MAR scanner 345 mm plate |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 82.863, 82.863, 174.419 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 74.850 - 1.800 |
| R-factor | 0.1684 |
| Rwork | 0.167 |
| R-free | 0.19580 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1yll |
| RMSD bond length | 0.023 |
| RMSD bond angle | 2.001 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 74.850 | 50.000 | 1.850 |
| High resolution limit [Å] | 1.790 | 3.860 | 1.790 |
| Rmerge | 0.037 | 0.029 | 0.290 |
| Number of reflections | 57596 | ||
| <I/σ(I)> | 35.11 | ||
| Completeness [%] | 98.9 | 99.9 | 88.7 |
| Redundancy | 9.3 | 15 | 6.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 291 | Ammonium formate |
