5UYF
YfeA from M9 minimal media supplemented with zinc - Mn wavelength
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-01-10 |
Detector | RAYONIX MX-300 |
Wavelength(s) | 1.89289 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 41.859, 52.191, 112.762 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.300 - 2.057 |
R-factor | 0.1662 |
Rwork | 0.162 |
R-free | 0.20040 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5uyd |
RMSD bond length | 0.006 |
RMSD bond angle | 0.766 |
Data reduction software | HKL-2000 (v712) |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.100 |
High resolution limit [Å] | 2.057 | 2.057 |
Rmerge | 0.093 | 0.411 |
Rpim | 0.037 | 0.171 |
Number of reflections | 15986 | 800 |
<I/σ(I)> | 67.3 | 13.5 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 7.2 | 6.9 |
CC(1/2) | 0.995 | 0.883 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.3 | 295.15 | 30% PEG 4000, 20mM Bis-tris propane, 50mM sodium chloride, 0.05% w/v sodium azide |