5UY4
YfeA from M9 minimal media supplemented with iron - Fe wavelength
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-01-10 |
Detector | RAYONIX MX-300 |
Wavelength(s) | 1.74013 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 61.930, 66.374, 67.154 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.207 - 1.915 |
R-factor | 0.1755 |
Rwork | 0.173 |
R-free | 0.20140 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5uy0 |
RMSD bond length | 0.007 |
RMSD bond angle | 0.805 |
Data reduction software | HKL-2000 (v712) |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.950 |
High resolution limit [Å] | 1.915 | 1.915 |
Rmerge | 0.063 | 0.414 |
Rpim | 0.024 | 0.155 |
Number of reflections | 21484 | 1046 |
<I/σ(I)> | 56 | 3.1 |
Completeness [%] | 98.0 | 96.1 |
Redundancy | 7.9 | 7.8 |
CC(1/2) | 0.997 | 0.934 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.3 | 293.15 | 30% PEG 4000, 20mM Bis-tris, 50mM sodium chloride, 0.05% w/v sodium azide |