5UWG
The crystal structure of Fz4-CRD in complex with palmitoleic acid
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-G |
Synchrotron site | APS |
Beamline | 21-ID-G |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-06-27 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 0.9786 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 103.452, 109.373, 76.789 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.830 - 2.560 |
R-factor | 0.2456 |
Rwork | 0.244 |
R-free | 0.26690 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5cm4 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.116 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.670 |
High resolution limit [Å] | 2.560 | 2.560 |
Rmerge | 0.041 | 1.000 |
Number of reflections | 14355 | 1739 |
<I/σ(I)> | 25.3 | 2 |
Completeness [%] | 99.8 | 100 |
Redundancy | 7.3 | 7.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 3.5 | 293 | 0.1 M citric acid pH 3.5, 28% w/v polyethylene glycol 8,000 |