5UV0
Crystal Structure of (+)-Limonene Synthase from Citrus sinensis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.2 |
Synchrotron site | ALS |
Beamline | 8.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-10-30 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 85.790, 85.790, 216.350 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.992 - 2.300 |
R-factor | 0.192 |
Rwork | 0.190 |
R-free | 0.22870 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2ong |
RMSD bond length | 0.007 |
RMSD bond angle | 0.819 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (dev_2294) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.300 |
Rmerge | 0.100 |
Number of reflections | 36820 |
<I/σ(I)> | 17.2 |
Completeness [%] | 99.8 |
Redundancy | 20.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 296 | 16% PEG8000, 100 mM Tris pH 7.5, 350 mM sodium tartrate |