5URD
wild type rat CYPOR bound with NADP+ - oxidized form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X26C |
Synchrotron site | NSLS |
Beamline | X26C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-11-03 |
Detector | DECTRIS PILATUS 300K |
Wavelength(s) | 1.1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 101.179, 114.929, 117.613 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.970 - 1.900 |
R-factor | 0.205 |
Rwork | 0.205 |
R-free | 0.23900 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.300 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | CNS (1.3) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.900 |
Number of reflections | 107662 |
<I/σ(I)> | 47 |
Completeness [%] | 100.0 |
Redundancy | 10.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 292 | PEG 4000, Sodium Acetate, HEPES |