5UQI
E. coli CFT073 c3406 in complex with A5P
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-D |
Synchrotron site | APS |
Beamline | 21-ID-D |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-06-13 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 0.9785 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 70.890, 71.830, 76.850 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 17.960 - 1.620 |
R-factor | 0.18106 |
Rwork | 0.180 |
R-free | 0.20117 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3fxa |
RMSD bond length | 0.018 |
RMSD bond angle | 1.997 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 17.960 |
High resolution limit [Å] | 1.620 |
Number of reflections | 24950 |
<I/σ(I)> | 6.58 |
Completeness [%] | 99.3 |
Redundancy | 6.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 294 | 0.1 M sodium citrate tribasic dehydrate pH 5.6, 0.5 M NaCl, 2% v/v ethylene imine polymer |