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5ULV

Malate dehydrogenase from Methylobacterium extorquens

Replaces:  4ROR
Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRL BEAMLINE BL7-1
Synchrotron siteSSRL
BeamlineBL7-1
Temperature [K]100
Detector technologyCCD
Collection date2014-07-10
DetectorADSC QUANTUM 315r
Wavelength(s)1.127092
Spacegroup nameP 64 2 2
Unit cell lengths108.995, 108.995, 104.659
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution37.750 - 1.660
R-factor0.14084
Rwork0.140
R-free0.16765
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3gvh
RMSD bond length0.020
RMSD bond angle1.909
Data reduction softwareiMOSFLM
Data scaling softwareAimless
Phasing softwarePHASER
Refinement softwareREFMAC (5.8.0135)
Data quality characteristics
 Overall
Low resolution limit [Å]37.750
High resolution limit [Å]1.660
Number of reflections44052
<I/σ(I)>14.2
Completeness [%]99.6
Redundancy11.2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7.529825-28% PEG400, 180-220mM CaCl2, 0.1M Hepes pH 7.5

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