5UIF
Crystal Structure of Native Ps01740
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.3 |
Synchrotron site | ALS |
Beamline | 5.0.3 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-02-21 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97648 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 80.722, 58.902, 84.759 |
Unit cell angles | 90.00, 110.37, 90.00 |
Refinement procedure
Resolution | 46.480 - 2.570 |
R-factor | 0.2218 |
Rwork | 0.219 |
R-free | 0.27160 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3n4g |
RMSD bond length | 0.002 |
RMSD bond angle | 0.464 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX (1.9_1692) |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 46.480 |
High resolution limit [Å] | 2.570 |
Number of reflections | 11402 |
<I/σ(I)> | 7.9 |
Completeness [%] | 96.0 |
Redundancy | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | 18% PEG 8000 0.1 M CHES pH 9.0 |