Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X8C |
| Synchrotron site | NSLS |
| Beamline | X8C |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2001-08-16 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 1.0094 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 217.200, 40.761, 75.460 |
| Unit cell angles | 90.00, 95.80, 90.00 |
Refinement procedure
| Resolution | 29.250 - 2.100 |
| R-factor | 0.2155 |
| Rwork | 0.213 |
| R-free | 0.26600 |
| Structure solution method | MAD |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.050 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | MLPHARE |
| Refinement software | BUSTER (2.10.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 64.550 | 2.180 |
| High resolution limit [Å] | 2.100 | 2.100 |
| Number of reflections | 37373 | |
| <I/σ(I)> | 21.7 | 3.5 |
| Completeness [%] | 94.5 | 84.3 |
| Redundancy | 3.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.7 | 298 | PEG 3350, SODIUM CHLORIDE, TRIS, PH 7.7, VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 298K |
