5UGW
STRUCTURE OF THE HUMAN TELOMERASE THUMB DOMAIN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-01-18 |
Detector | RIGAKU SATURN 944 |
Wavelength(s) | 1.54178 |
Spacegroup name | P 3 2 1 |
Unit cell lengths | 92.425, 92.425, 50.178 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 26.680 - 2.310 |
R-factor | 0.19781 |
Rwork | 0.197 |
R-free | 0.20900 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.186 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 26.680 | 2.360 |
High resolution limit [Å] | 2.300 | 2.300 |
Number of reflections | 10654 | 813 |
<I/σ(I)> | 18.68 | 2.19 |
Completeness [%] | 99.8 | 98.3 |
Redundancy | 10.8 | 10.25 |
CC(1/2) | 0.999 | 0.700 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 283 | 50 mM Tris 8.5 0.8 M LiSo4 10 mM GSH/GSSG 3% 1,6-hexanediol |