5UFR
Structure of RORgt bound to
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2015-09-26 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 104.089, 107.053, 124.122 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.717 - 2.068 |
R-factor | 0.2192 |
Rwork | 0.217 |
R-free | 0.25350 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.760 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.000 |
Number of reflections | 42514 |
<I/σ(I)> | 27.2 |
Completeness [%] | 99.7 |
Redundancy | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 1.4M NaAcetate, 100mM MES pH 6.5 |