5UFR

Structure of RORgt bound to

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	80
Detector technology	PIXEL
Collection date	2015-09-26
Detector	DECTRIS PILATUS 6M
Wavelength(s)	1
Spacegroup name	C 2 2 21
Unit cell lengths	104.089, 107.053, 124.122
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	47.717 - 2.068
R-factor	0.2192
Rwork	0.217
R-free	0.25350
RMSD bond length	0.006
RMSD bond angle	0.760
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX ((1.10_2155: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.000
Number of reflections	42514
<I/σ(I)>	27.2
Completeness [%]	99.7
Redundancy	6.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		293	1.4M NaAcetate, 100mM MES pH 6.5