5UF8
Crystal structure of the ARF family small GTPase ARF2 from Candida albicans in complex with GDP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2016-12-13 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 |
Unit cell lengths | 38.289, 64.362, 79.236 |
Unit cell angles | 78.11, 83.73, 72.77 |
Refinement procedure
Resolution | 24.873 - 1.872 |
R-factor | 0.2364 |
Rwork | 0.235 |
R-free | 0.26980 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1mr3 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.647 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | BALBES |
Refinement software | PHENIX ((dev_2481: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 1.910 |
High resolution limit [Å] | 1.880 | 1.880 |
Rmerge | 0.054 | 0.409 |
Number of reflections | 53906 | |
<I/σ(I)> | 41.35 | 5.04 |
Completeness [%] | 93.4 | 90.7 |
Redundancy | 4.1 | 4.3 |
CC(1/2) | 0.838 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 298 | 30% PEG2K MME, 0.2 M ammonium sulfate, 0.1 M sodium acetate pH 4.6, 5 mM magnesium chloride, 5 mM ADP |