5UE3
proMMP-9desFnII
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-03-05 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 90.300, 73.200, 77.500 |
Unit cell angles | 90.00, 106.30, 90.00 |
Refinement procedure
Resolution | 32.840 - 1.599 |
R-factor | 0.1575 |
Rwork | 0.154 |
R-free | 0.18380 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.240 |
Data reduction software | d*TREK |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 49.190 |
High resolution limit [Å] | 1.599 |
Rmerge | 0.048 |
Number of reflections | 62722 |
<I/σ(I)> | 13.4 |
Completeness [%] | 98.1 |
Redundancy | 3.19 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 5.5 | 293 | 25% PEG 8K 1% glycerol 0.2 M ammonium sulfate 100 mM NaCacodylate |