5U91
Crystal structure of Tre/loxLTR complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.2 |
Synchrotron site | ALS |
Beamline | 8.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-12-03 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97918 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 70.260, 193.390, 89.020 |
Unit cell angles | 90.00, 111.25, 90.00 |
Refinement procedure
Resolution | 82.967 - 3.104 |
R-factor | 0.2112 |
Rwork | 0.209 |
R-free | 0.25300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1q3u |
RMSD bond length | 0.004 |
RMSD bond angle | 0.639 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (dev_1839) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 96.690 |
High resolution limit [Å] | 3.100 |
Number of reflections | 71563 |
<I/σ(I)> | 3.9 |
Completeness [%] | 90.7 |
Redundancy | 4.2 |
CC(1/2) | 0.951 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | 10 mM sodium citrate, 25-32.5 % Peg 6000 |