5U85
Murine saposin-D (SapD), open conformation
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-11-30 |
Detector | RAYONIX MX-300 |
Wavelength(s) | 0.97949 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 41.650, 43.163, 88.822 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.822 - 1.650 |
R-factor | 0.1672 |
Rwork | 0.166 |
R-free | 0.18570 |
Structure solution method | AB INITIO PHASING |
RMSD bond length | 0.003 |
RMSD bond angle | 0.665 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | ACORN |
Refinement software | PHENIX ((1.10.1_2155)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.650 |
Number of reflections | 19863 |
<I/σ(I)> | 33.2 |
Completeness [%] | 100.0 |
Redundancy | 7.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | sodium citrate PEG 4000 isopropanol |