5TUR
Pim-1 kinase in complex with a 7-azaindole
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-F |
Synchrotron site | APS |
Beamline | 21-ID-F |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-02-01 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 1.00 |
Spacegroup name | P 65 |
Unit cell lengths | 97.747, 97.747, 80.792 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 37.492 - 2.948 |
R-factor | 0.2087 |
Rwork | 0.204 |
R-free | 0.24780 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.668 |
Refinement software | PHENIX ((1.11_2567: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 37.492 |
High resolution limit [Å] | 2.948 |
Number of reflections | 9343 |
<I/σ(I)> | 2.69 |
Completeness [%] | 99.8 |
Redundancy | 13 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 277 | 0.1M imidazole, 1M NaAcetate, 20% glycerol pH 6.5 |