5TUB
Crystal Structure of the Shark TBC1D15 GAP Domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-D |
Synchrotron site | APS |
Beamline | 21-ID-D |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-06-02 |
Detector | MARRESEARCH |
Wavelength(s) | 1.0 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 224.790, 149.740, 95.030 |
Unit cell angles | 90.00, 108.93, 90.00 |
Refinement procedure
Resolution | 47.260 - 2.850 |
R-factor | 0.2171 |
Rwork | 0.215 |
R-free | 0.24770 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5tuc |
RMSD bond length | 0.006 |
RMSD bond angle | 0.984 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.260 | 2.920 |
High resolution limit [Å] | 2.850 | 2.850 |
Rmerge | 0.141 | 1.165 |
Number of reflections | 69398 | |
<I/σ(I)> | 10.7 | 1.7 |
Completeness [%] | 100.0 | |
Redundancy | 7.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7 | 293 | 1.35 M ammonium sulfate, 0.09 M BIS-TRIS propane (pH 7.0) and 0.01 M calcium chloride dehydrate |