5TO5
Structure of the TPR oligomerization domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-D |
Synchrotron site | APS |
Beamline | 21-ID-D |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-03-16 |
Detector | RAYONIX MX300-HS |
Wavelength(s) | 1.07812 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 74.177, 51.551, 94.980 |
Unit cell angles | 90.00, 107.83, 90.00 |
Refinement procedure
Resolution | 21.411 - 2.500 |
R-factor | 0.2318 |
Rwork | 0.229 |
R-free | 0.28200 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.722 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 21.850 |
High resolution limit [Å] | 2.180 |
Rmerge | 0.079 |
Number of reflections | 17251 |
<I/σ(I)> | 15.8 |
Completeness [%] | 96.0 |
Redundancy | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 6.25 | 295 | 16% PEG1.5K, 0.1M Bistris (6.25) |