5TKN
Crystal structure of FBP aldolase from Toxoplasma gondii, Schiff base FBP complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X25 |
Synchrotron site | NSLS |
Beamline | X25 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-03-27 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.1 |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 109.100, 109.100, 54.671 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.275 - 1.920 |
R-factor | 0.1544 |
Rwork | 0.150 |
R-free | 0.19880 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.005 |
RMSD bond angle | 0.923 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.850 |
High resolution limit [Å] | 1.820 | 4.940 | 1.820 |
Rmerge | 0.069 | 0.054 | |
Total number of observations | 188737 | ||
Number of reflections | 22332 | ||
<I/σ(I)> | 11.3 | ||
Completeness [%] | 73.8 | 99.8 | 13.3 |
Redundancy | 8.5 | 11.9 | 1.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 296 | 0.1M Sodium Acetate, 0.2M Lithium Sulfate, 3.5% PEG 8000, 10% PEG 1000 |