5TKG
Neurospora crassa polysaccharide monooxygenase 2 resting state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-12-03 |
Detector | RAYONIX MX300-HS |
Wavelength(s) | 1.000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 67.350, 42.210, 69.480 |
Unit cell angles | 90.00, 98.96, 90.00 |
Refinement procedure
Resolution | 31.950 - 1.200 |
R-factor | 0.1138 |
Rwork | 0.113 |
R-free | 0.14000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4eir |
RMSD bond length | 0.009 |
RMSD bond angle | 1.184 |
Data reduction software | MOSFLM (7.2.1) |
Data scaling software | Aimless (0.5.27) |
Phasing software | PHASER (2.6.0) |
Refinement software | PHENIX (1.10.1-2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.640 | 1.220 |
High resolution limit [Å] | 1.200 | 1.200 |
Rmerge | 0.117 | 0.251 |
Rmeas | 0.140 | |
Rpim | 0.076 | |
Total number of observations | 400665 | |
Number of reflections | 117131 | |
<I/σ(I)> | 7.1 | |
Completeness [%] | 97.0 | 95 |
Redundancy | 3.4 | 3.4 |
CC(1/2) | 0.978 | 0.914 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6 | 295 | PEG 3350, HEPES |