5TJF

The crystal structure of Allophycocyanin from the red algae Gracilaria chilensis

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SOLEIL BEAMLINE PROXIMA 1
Synchrotron site	SOLEIL
Beamline	PROXIMA 1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2016-02-27
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.9786
Spacegroup name	P 3 2 1
Unit cell lengths	97.410, 97.410, 63.830
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	42.180 - 2.300
R-factor	0.2584
Rwork	0.257
R-free	0.28390
RMSD bond length	0.004
RMSD bond angle	1.555
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	42.180	2.382
High resolution limit [Å]	2.300	2.300
Rmerge	0.130	0.357
Number of reflections	29513
<I/σ(I)>	8.43
Completeness [%]	97.0	97
Redundancy	2.9	2.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7	291	18% PEG 6000 0.3 M NaCl 0.1 M MES