5TJF
The crystal structure of Allophycocyanin from the red algae Gracilaria chilensis
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SOLEIL BEAMLINE PROXIMA 1 |
| Synchrotron site | SOLEIL |
| Beamline | PROXIMA 1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-02-27 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.9786 |
| Spacegroup name | P 3 2 1 |
| Unit cell lengths | 97.410, 97.410, 63.830 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 42.180 - 2.300 |
| R-factor | 0.2584 |
| Rwork | 0.257 |
| R-free | 0.28390 |
| RMSD bond length | 0.004 |
| RMSD bond angle | 1.555 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 42.180 | 2.382 |
| High resolution limit [Å] | 2.300 | 2.300 |
| Rmerge | 0.130 | 0.357 |
| Number of reflections | 29513 | |
| <I/σ(I)> | 8.43 | |
| Completeness [%] | 97.0 | 97 |
| Redundancy | 2.9 | 2.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 291 | 18% PEG 6000 0.3 M NaCl 0.1 M MES |
