5TH1
Crystal structure of H10 hemagglutinin mutant (K158aA-Q226L-G228S) from Jiangxi-Donghu (2013) H10N8 influenza virus in complex with 6'-SLNLN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-05-14 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97950 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 64.404, 254.466, 70.649 |
Unit cell angles | 90.00, 112.03, 90.00 |
Refinement procedure
Resolution | 48.820 - 2.191 |
R-factor | 0.192 |
Rwork | 0.190 |
R-free | 0.22940 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5tgo |
RMSD bond length | 0.016 |
RMSD bond angle | 2.566 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.230 |
High resolution limit [Å] | 2.190 | 2.190 |
Number of reflections | 105198 | |
<I/σ(I)> | 27 | 4.4 |
Completeness [%] | 97.9 | |
Redundancy | 3.7 | 3.6 |
CC(1/2) | 0.875 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 293.15 | 0.2 M NaCl, 10% (w/v) PEG 8000, 0.1M CHES pH 9.5 |