5TAO
Haloferax volcanii Malate Synthase Lead(II) complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2009-03-15 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.54 |
Spacegroup name | H 3 2 |
Unit cell lengths | 155.353, 155.353, 139.412 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 96.810 - 2.100 |
R-factor | 0.18477 |
Rwork | 0.183 |
R-free | 0.21668 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3pug |
RMSD bond length | 0.020 |
RMSD bond angle | 1.916 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER (2.5.5) |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 96.810 | 30.000 | 2.180 |
High resolution limit [Å] | 2.100 | 4.520 | 2.100 |
Rmerge | 0.103 | 0.099 | 0.374 |
Number of reflections | 35791 | ||
<I/σ(I)> | 13.2 | ||
Completeness [%] | 99.5 | 96.3 | 100 |
Redundancy | 3.7 | 3.9 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | magnesium chloride, glyoxylate, Tris, KCl, ammonium acetate, PEG 4500, glycerol, sodium acetate trihydrate |