5T6Z
KIR3DL1 in complex with HLA-B*57:01-TW10
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-05-11 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.954 |
Spacegroup name | P 1 |
Unit cell lengths | 51.812, 61.382, 65.359 |
Unit cell angles | 95.31, 98.02, 109.23 |
Refinement procedure
Resolution | 39.870 - 2.000 |
R-factor | 0.205 |
Rwork | 0.203 |
R-free | 0.24000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3vh8 |
RMSD bond length | 0.005 |
RMSD bond angle | 1.142 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.7.2_869) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.867 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.082 | 0.218 |
Number of reflections | 47511 | |
<I/σ(I)> | 11.2 | 11.2 |
Completeness [%] | 94.4 | 94.2 |
Redundancy | 4.9 | 4.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 298 | 16% PEG 3350, 2% tacsimate pH 5.0 and 0.1M tri-sodium citrate pH 5.6 |