5T6W
HLA-B*57:01 presenting SSTRGISQLW
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-04-12 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.954 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 50.790, 81.180, 109.790 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.637 - 1.900 |
R-factor | 0.2139 |
Rwork | 0.211 |
R-free | 0.26300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2rfx |
RMSD bond length | 0.007 |
RMSD bond angle | 1.044 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.637 | 2.000 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.197 | 0.553 |
Number of reflections | 36411 | |
<I/σ(I)> | 4.7 | 2.3 |
Completeness [%] | 99.6 | 99.8 |
Redundancy | 3.9 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 298 | 12 -20 % PEG 4000, 0.2 M ammonium acetate and 0.1 M tri-sodium citrate pH 5.6 |