5T65
LIGAND BINDING DOMAIN OF PSEUDOMONAS AERUGINOSA PAO1 AMINO ACID CHEMORECEPTOR PCTA IN COMPLEX WITH L-ILE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-11-25 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.9801 |
Spacegroup name | P 61 |
Unit cell lengths | 132.610, 132.610, 77.090 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 33.153 - 2.200 |
R-factor | 0.1681 |
Rwork | 0.166 |
R-free | 0.20380 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3c8c |
RMSD bond length | 0.010 |
RMSD bond angle | 1.162 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 33.153 | 2.280 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.060 | 0.540 |
Number of reflections | 39288 | |
<I/σ(I)> | 20.99 | 3.32 |
Completeness [%] | 100.0 | 100 |
Redundancy | 7 | 7 |
CC(1/2) | 0.999 | 0.866 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIQUID DIFFUSION | 5 | 293.5 | Capillary COUNTER-DIFFUSION: 2.8 M AMMONIUM SULPHATE, 0.1M SODIUM ACETATE pH 5.0, T 20 C |