5T3R

Crystal structure of BT1762-1763

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I24
Synchrotron site	Diamond
Beamline	I24
Temperature [K]	100
Detector technology	PIXEL
Collection date	2015-10-10
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.9686
Spacegroup name	P 21 21 2
Unit cell lengths	151.770, 117.330, 119.890
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	75.885 - 3.100
R-factor	0.2005
Rwork	0.197
R-free	0.25940
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.010
RMSD bond angle	1.275
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	75.900
High resolution limit [Å]	2.820
Number of reflections	52316
<I/σ(I)>	5
Completeness [%]	99.9
Redundancy	7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	0.1 M magnesium formate dihydrate, 0.1 M MOPS pH 7, 17% w/v PEG3350