5T3B
Crystal structure of BpGH50
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-07-04 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.92017 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 73.100, 87.370, 74.670 |
Unit cell angles | 90.00, 105.50, 90.00 |
Refinement procedure
Resolution | 71.950 - 1.400 |
R-factor | 0.1076 |
Rwork | 0.106 |
R-free | 0.14540 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.019 |
RMSD bond angle | 1.802 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 71.950 | 1.420 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.067 | 0.451 |
Number of reflections | 176279 | |
<I/σ(I)> | 15.9 | 3.9 |
Completeness [%] | 99.3 | 95.6 |
Redundancy | 6.1 | 5 |
CC(1/2) | 0.998 | 0.844 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 291 | 17-25% PEG 3350, 0.04-0.1M Bis-Tris |