5T30
Human MnSOD-azide complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2016-02-02 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 77.900, 77.900, 238.442 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 67.460 - 1.770 |
R-factor | 0.21 |
Rwork | 0.209 |
R-free | 0.23900 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.333 |
Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 67.500 | 1.800 |
High resolution limit [Å] | 1.770 | 1.770 |
Number of reflections | 40981 | |
<I/σ(I)> | 12.7 | 2 |
Completeness [%] | 96.0 | 84 |
Redundancy | 5.6 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.8 | 296 | 1.8M potassium phosphate, pH 7.8 |