5T2X

Crystal structure of Uncharacterised protein lpg1670

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 19-BM
Synchrotron site	APS
Beamline	19-BM
Temperature [K]	100
Detector technology	CCD
Collection date	2013-08-20
Detector	ADSC QUANTUM 210r
Wavelength(s)	0.97952
Spacegroup name	C 2 2 21
Unit cell lengths	138.922, 238.831, 100.495
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	27.661 - 2.303
R-factor	0.2114
Rwork	0.210
R-free	0.23380
Structure solution method	SAD
RMSD bond length	0.001
RMSD bond angle	0.412
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Phasing software	HKL-3000
Refinement software	PHENIX ((dev_2386: ???))

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	50.000	50.000	2.320
High resolution limit [Å]	2.280	6.190	2.280
Rmerge	0.102	0.056	0.792
Rmeas	0.108	0.059	0.838
Rpim	0.034	0.020	0.267
Total number of observations	670803
Number of reflections	71709
<I/σ(I)>	9.5
Completeness [%]	98.0	95.7	95.5
Redundancy	9.4	8.5	9.1
CC(1/2)		0.997	0.897

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7	298	0.1M Bis-Tris, 3.5M Sodium formate