Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

5T2M

mPI3Kd IN COMPLEX WITH 7m

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID23-1
Synchrotron siteESRF
BeamlineID23-1
Temperature [K]100
Detector technologyCCD
Collection date2013-05-13
DetectorADSC QUANTUM 315
Wavelength(s)0.976
Spacegroup nameC 2 2 21
Unit cell lengths63.577, 141.782, 219.178
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution59.520 - 2.800
R-factor0.23
Rwork0.228
R-free0.27000
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.008
RMSD bond angle0.960
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwareMOLREP
Refinement softwareBUSTER (2.11.6)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]219.1802.950
High resolution limit [Å]2.8002.800
Rmerge0.1700.672
Number of reflections24681
<I/σ(I)>7.42.2
Completeness [%]99.195.8
Redundancy5.85
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP29350% ethylene glycol/PEG 8000, 0.1 M carboxylic acids mix, 0.1 M Buffer system 2 pH 7.5

226707

PDB entries from 2024-10-30

PDB statisticsPDBj update infoContact PDBjnumon