5T21
CRYSTAL STRUCTURE OF HSP90 IN COMPLEX WITH SAR148019.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-04-01 |
Detector | MARRESEARCH |
Wavelength(s) | 1.54 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 66.920, 98.580, 90.860 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.620 - 2.100 |
R-factor | 0.174 |
Rwork | 0.172 |
R-free | 0.21600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2yk2 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.040 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | BUSTER (2.11.7) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 19.620 |
High resolution limit [Å] | 2.100 |
Number of reflections | 16887 |
<I/σ(I)> | 15.4 |
Completeness [%] | 100.0 |
Redundancy | 7.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 1.0 to 1.4M Sodium Citrate |