5T1O
Solution-state NMR and SAXS structural ensemble of NPr (1-85) in complex with EIN-Ntr (170-424)
Spectrometer
Experimental method: SOLUTION NMR, SOLUTION SCATTERING
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | AVANCE | 600 | |
| 2 | Bruker | AVANCE | 800 | |
| 3 | Bruker | AVANCE | 900 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 3D HN(CO)CACB TROSY |
| 10 | 1 | 2 | 3D 1H-15N NOESY TROSY |
| 11 | 1 | 2 | 3D HN(CO)CACB TROSY |
| 12 | 1 | 2 | 3D HNCACB TROSY |
| 13 | 1 | 2 | 3D HNCA TROSY |
| 14 | 1 | 6 | 3D HNCACB |
| 15 | 1 | 1 | ARTSY |
| 16 | 1 | 2 | ARTSY |
| 17 | 1 | 3 | ARTSY |
| 18 | 1 | 4 | ARTSY |
| 19 | 1 | 8 | 2D 1H-15N HSQC TROSY |
| 2 | 1 | 1 | 3D HN(CA)CO TROSY |
| 20 | 1 | 9 | 2D 1H-15N HSQC TROSY |
| 21 | 1 | 10 | 2D 1H-15N HSQC TROSY |
| 22 | 1 | 11 | 2D 1H-15N HSQC TROSY |
| 3 | 1 | 1 | 3D HNCACB TROSY |
| 4 | 1 | 1 | 3D 1H-15N NOESY TROSY |
| 7 | 1 | 1 | 3D HNCO TROSY |
| 8 | 1 | 1 | 3D HNCA TROSY |
| 9 | 1 | 5 | 3D HNCA TROSY |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 7.5 | 1 | 300 |
Conformers
| Conformers Calculated Total Number | 200 |
| Conformers Submitted Total Number | 20 |
Refinement Statistics
Experimental method: SOLUTION NMR, SOLUTION SCATTERING
| Cell axes | |||
| Cell angles | |||
| Spacegroup | |||
| Resolution limits | - | ||
